Operation and Calibration of (VACUUM OVEN CINTEX CIC 61)

Basic Operation: Before using the Vacuum oven, check the validity of calibration. Switch on the instrument by the “MAINS” switch on the control panel of the instrument. The control panel consists of Microprocessor based Temperature controller, Three heat control switch (Rotatory switch) to control heating rate control, Fuse, Vacuum gauge.
To set the desired temperature press set key on Microprocessor based Temperature controller until SP is displayed. Press enter. Usage of “Three heat control switch” – based upon he target set temperature he rotator. switch should be set as follows.
Temperature controller, Microprocessor, instrument, Vacuum

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Table of contents (toc) for republic of uzbekistan

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Preparation of mercuric acetate solution 10 percent

Pour about 75 ml of Glacial Acetic Acid into a 250 ml capacity beaker. Weigh 10.0 grams of Mercuric Acetate LR and transfer slowly, into above-said beaker, though it‘s sidewalls, while gentle mixing by using a glass rod. Transfer prepared solution into a 100 ml volumetric flask, by using a glass funnel. Rinse the beaker and funnel with few ml of Glacial Acetic Acid, and allow to add into the contents of volumetric flask. Make up the volumetric flask to mark with Glacial Acetic Acid , remove the funnel, keep the lid to close the volumetric flask and shake gently to mix the solution. Transfer the prepared solution into a suitable container and label with all necessary details. The resultant solution is having the concentration of 10.0% w/v. Mercuric Acetate , Glacial Acetic Acid , Glass funnel, Volumetric flask

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